反応 #362166

反応方程式

indene

sodium

→

Indene Sodium Salt

溶媒

tetrahydrofuran

反応条件

後処理

1. 1
   その他reaction
2. 2
   温度at reflux for 4 hours
3. 3
   その他Thereafter, unreacted sodium was removed
4. 4
   その他a 2 mols/l THF solution was prepared

実験手順

50 ml of purified tetrahydrofuran (THF) was charged into a three-necked 300 ml flask, then 20 g of indene and 4 g of metal sodium were added, and reaction was allowed to take place at reflux for 4 hours. Thereafter, unreacted sodium was removed and then a 2 mols/l THF solution was prepared using the reaction product.

出典