反応 #359159

反応方程式

trimethylchlorosilane

2-bromoindene

magnesium

→

Bromomagnesium indene

2-trimethylsilylindene

反応条件

実験手順

Bromomagnesium indene was prepared from 10.0 g (51.3 mmol) of 2-bromoindene and 5 g of magnesium in a nitrogen stream. The reaction product was reacted with 6.5 ml of trimethylchlorosilane to obtain 7.14 g (37.9 mmol) of 2-trimethylsilylindene as a colorless oily product.

出典