反応 #359072
ord-321efd9e941f4a5a9155c968db9dec32
反応方程式
反応条件
詳細条件
See reaction.notes.procedure_details.
後処理
- 1その他the volatiles were removed in vacuo
実験手順
N-(3-Azido-5-fluoropyridin-2-yl)-2,2-dimethylpropanamide (275 mg, 1.16 mmol) in 3 N HCl (5 mL) was heated to 100° C. After 2 h, the volatiles were removed in vacuo, to give the title compound as its HCl salt (180 mg). MS 154.2 (M+1).