反応 #359072

ord-321efd9e941f4a5a9155c968db9dec32

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他the volatiles were removed in vacuo

実験手順

N-(3-Azido-5-fluoropyridin-2-yl)-2,2-dimethylpropanamide (275 mg, 1.16 mmol) in 3 N HCl (5 mL) was heated to 100° C. After 2 h, the volatiles were removed in vacuo, to give the title compound as its HCl salt (180 mg). MS 154.2 (M+1).

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US07452903B2uspto-grants-2008_11