反応 #354749

反応方程式

ammonia

trimethylchlorosilane

6-bromohexan-1-ol

→

ammonia

6-bromohexyloxytrimethylsilane

溶媒

benzene

反応条件

実験手順

13.8 G. of trimethylchlorosilane and 11.4 g. of 6-bromohexan-1-ol are mixed together in 100 ml. of dry benzene and are stirred in an ice-bath while anhydrous ammonia is passed therethrough until the odor of ammonia persists to obtain 6-bromohexyloxytrimethylsilane, which is worked up by filtration, followed by evaporation of the filtrate and distillation in vacuo.

出典