反応 #352386

ord-9e9d153470d04be5bb31457535a9d24b

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

236faE (CAS Reg. No. 20193-67-3) has been prepared by reaction of 2,2,2-trifluoroethanol with carbonyl fluoride to give the intermediate, CF3CH2OCOF, which was in mm reacted with sulfur tetrafluoride at 150°-200° C. to give the product as disclosed by Eisemann in U.S. Pat. No. 3,394,878.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US05648016uspto-grants-1997_07