反応 #351013

反応方程式

( a )

2,3-difluoro-4'-[6-(acryloyloxy)hexyloxy]biphenyl

8-bromo-1-octanol

6-bromo-1-hexanol

→

8-acryloyloxy-1-bromooctane

収率 78.0%

反応条件

実験手順

The same procedure as in the synthesis (a) of Example 2 was repeated except that 34.7 g of 8-bromo-1-octanol were used instead of 30 g of 6-bromo-1-hexanol to give 34.1 g (Y., 78%) of 8-acryloyloxy-1-bromooctane. GC; 97%

出典