反応 #350363

ord-94117af54e3342ffb32829457d06bb7d

反応方程式

NC1CCCc2sccc21
4,5,6,7-tetrahydrobenzo[b]thiophen-4-amine
CCCCCCN=C=O
n-hexyl isocyanate
CCCCCCNC(=O)NC1CCCc2sccc21
1-(n-hexyl)-3-(4,5,6,7-tetrahydrobenzo[b]thien-4-yl)urea

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

In the manner described in Example 1, 4,5,6,7-tetrahydrobenzo[b]thiophen-4-amine is allowed to react with n-hexyl isocyanate to give 1-(n-hexyl)-3-(4,5,6,7-tetrahydrobenzo[b]thien-4-yl)urea, melting point 122° C. to 124° C.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US04156670uspto-grants-1979_05