反応 #3489

反応方程式

4-(3-acetylphenyl)amino-2-amino-6methylpyrimidine

methyl iodide

→

4-(3-acetylphenyl)amino-2-amino-1,6-dimethylpyrimidinium iodide

溶媒

acetone

反応条件

後処理

1. 1
   温度was heated
2. 2
   温度at reflux for 48 hr
3. 3
   ろ過Filtration
4. 4
   温度after cooling

実験手順

Compound No. 14: 4-(3-acetylphenyl)amino-2-amino-6methylpyrimidine, Compound No. 15, (0.968 g) was suspended in acetone (5 mL) containing methyl iodide (2 mL) was heated at reflux for 48 hr. Filtration after cooling gave 0.657 g of 4-(3-acetylphenyl)amino-2-amino-1,6-dimethylpyrimidinium iodide as a white powder, mp 238°-40° C.

出典