反応 #347746

ord-87750b6dcbd94ff195e4a634e9e04e77

反応方程式

COc1ccc(C=O)cc1
p-methoxy benzaldehyde
COC(C)=O
methyl acetate
COC(=O)C=Cc1ccc(OC)cc1
methyl p-methoxycinnamate
COc1ccc(C=CC(=O)O)cc1
p-methoxycinnamic acid

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

The process of claim 1 wherein p-methoxy benzaldehyde is reacted with methyl acetate in step (a); methyl p-methoxycinnamate is formed in step (b) and methyl p-methoxycinnamate and p-methoxycinnamic acid are reacted with a C8 alkanol in step (e) to produce a C8 alkyl p-methoxycinnamate as the product of the process.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US05527947uspto-grants-1996_06