反応 #347136

反応方程式

tetrafluorophthalic anhydride

methanol

methanol

→

3,4,5,6-tetrafluorophthalic acid-monomethyl ester

収率 98.0%

反応条件

後処理

1. 1
   その他Into a 100 ml glass reactor equipped with a reflux condenser and a stirrer
2. 2
   温度under reflux
3. 3
   workup.DISTILLATIONwas distilled off

実験手順

Into a 100 ml glass reactor equipped with a reflux condenser and a stirrer, 20 g (0.091 mol) of the tetrafluorophthalic anhydride prepared in Example 3 and 40 ml of methanol were charged, and the mixture was stirred for 2 hours under reflux. After completion of the reaction, methanol was distilled off to obtain 22.5 g of 3,4,5,6-tetrafluorophthalic acid-monomethyl ester. The yield was 98.0%.

出典