反応 #334978

反応方程式

n-decyl alcohol

naphthalene-2,6-dicarboxylic acid dichloride

triethylamine

dimethylaminopyridine

→

titled compound

収率 56.3%

2-n-decyloxycarbonylnaphthalene-6-carboxylic acid chloride

収率 56.3%

溶媒

methylene chloride

反応条件

後処理

1. 1
   workup.DISTILLATIONthe solution was distilled
2. 2
   その他to remove the solvent

実験手順

After a solution of n-decyl alcohol (0.5 g), naphthalene-2,6-dicarboxylic acid dichloride (0.6 g), and triethylamine (0.27 g) and a very small amount of dimethylaminopyridine in methylene chloride (50 ml) was stirred at room temperature overnight, the solution was distilled to remove the solvent, until the titled compound (about 0.5 g) was obtained.

出典