反応 #334230

反応方程式

3,5 dimethylpiperidine

4-chlorobutyronitrile

→

4-(3,5-dimethylpiperidino)-butyronitrile

溶媒

benzene

反応条件

後処理

1. 1
   workup.WAITare run in25 minutes

実験手順

Into a solution under reflux of 50 g (0.424 mole) of 3,5 dimethylpiperidine at 96% in 60 ml benzene are run in25 minutes 22 g (0.212 mole) of 4-chlorobutyronitrile and the reflux is continued for 2h.

出典