反応 #324820

ord-f3ef43ef2dca4acd8ad53bdc9f523824

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

The title compound is prepared from 2-methyl-pyridine-5-boronic acid and 2-bromo-5-iodo-1,3-dimethyl-benzene following a procedure analogous to that described in Step 1 of Intermediate 56. LC (method 9): tR=0.93 min; Mass spectrum (ESI+): m/z=276/278 (Br) [M+H]+.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US08642585B2uspto-grants-2014_02