反応 #324757

ord-2211b2ef377a493590653dd29b430aa5

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

The title compound is prepared from 2-bromo-5-iodo-1,3-dimethylbenzene and 1-methyl-2-oxo-1,2-dihydropyridin-4-ylboronic acid following a procedure analogous to that described in Step 1 of Intermediate 56. LC (method 11): tR=1.04 min; Mass spectrum (ESI+): m/z=292, 294 [M+H]+.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US08642585B2uspto-grants-2014_02