反応 #324358

反応方程式

aniline

propane sultone

→

3-phenylammonio-1-propanesulfonate

収率 95.0%

溶媒

acetonitrile

反応条件

後処理

1. 1
   ろ過the solid of 3-phenylammonio-1-propanesulfonate was filtered
2. 2
   その他air-dried

実験手順

A mixture of aniline (7 mmol) and propane sultone (10 mmol) was heated in 10 mL of acetonitrile at 12.0-130° C. for 9 h in a pressure tube under argon atmosphere. The product was allowed to cool to room temperature and the solid of 3-phenylammonio-1-propanesulfonate was filtered and air-dried. Yield: 95%.

出典