反応 #322838

ord-7337fbbc99fe4ec18e8d3211ccc24bea

反応方程式

Cl.NCCCl
2-chloroethylamine hydrochloride
Cl.O=S(=O)(Cl)c1ccc(Nc2cnnc3cc(Cl)ccc23)cc1
4-(7-chloro-4-cinnolinylamino)benzenesulphonyl chloride hydrochloride
O=S(=O)(NCCCl)c1ccc(Nc2cnnc3cc(Cl)ccc23)cc1
4-(7-Chloro-4-cinnolinylamino)-N-(2-chloroethyl) benzenesulphonamide

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

This compound is prepared in a similar manner to the procedure of Example 10 using equimolar quantities of 2-chloroethylamine hydrochloride instead of 3-chloropropylamine hydrochloride and 4-(7-chloro-4-cinnolinylamino)benzenesulphonyl chloride hydrochloride instead of 4-(7-chloro-4-quinolinylamino) benzenesulphonyl chloride.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US04640920uspto-grants-1987_02