反応 #321557

ord-24e07600bc1c4ee89c7bcac5adceca1e

反応方程式

COc1ccc(B(O)O)cc1
4-methoxyphenylboronic acid
O=S(=O)(c1ccc(Br)s1)n1cccc1
N-(5-bromothiophene-2-sulfonyl)pyrrole
COc1ccc(-c2ccc(S(=O)(=O)n3cccc3)s2)cc1
N-[5-(4-methoxyphenyl)thiophene-2-sulfonyl]pyrrole

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他Recrystallization
  2. 2
    その他gave a solid in quantative yield

実験手順

N-[5-(4-methoxyphenyl)thiophene-2-sulfonyl]pyrrole was prepared, in the same manner as described in Example 32C, from 4-methoxyphenylboronic acid and N-(5-bromothiophene-2-sulfonyl)pyrrole. Recrystallization using hexane/ethyl acetate gave a solid in quantative yield.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US05594021uspto-grants-1997_01