反応 #321554

ord-f4509aa58e704c21a3b7b244031cc66e

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他This was purified by recrystallization

実験手順

N-[5-(3-methoxyphenyl)thiophene-2-sulfonyl]pyrrole was prepared in the same manner as described in Example 32C from 3-methoxyphenylboronic acid and N-(5-bromothiophene-2-sulfonyl)pyrrole in 93% yield. This was purified by recrystallization using hexane/ethyl acetate as solvent.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US05594021uspto-grants-1997_01