反応 #319054

反応方程式

DCTA bromide

DMF

triethylamine

acetic

→

DCTA

溶媒

oxygen

反応条件

後処理

1. 1
   その他After reaction the mixture

実験手順

One millimole of DCTA-bromide was added to 5 ml of DMF containing 0.2 ml of 1,2-dithioethylene and 0.5 ml of triethylamine. The mixture was incubated under argon for 2 hours at 60°-70° C. After reaction the mixture was diluted with oxygen-free H2O to 50 ml, the pH was adjusted to 4.0-4.5 with glacial acetic

出典