反応 #312586
ord-ea8c19d0e5e54c419d16d402346fc712
反応条件
詳細条件
See reaction.notes.procedure_details.
後処理
- 1その他separated into two layers
実験手順
6.2 g (0.05 mole) of thioanisole and 6.9 g (0.055 mole) of dimethyl sulfate were stirred for 12 hours at room temperature. 100 g of water and 50 ml of diethyl ether were added to the reaction solution whereupon the mixture separated into two layers. The aqueous layer was taken out, which was an aqueous solution of the target compound, dimethylphenylsulfonium sulfate.