反応 #312577

反応方程式

Hydroxycarbonylmethyl methacrylate

dihydroxyadamantane

p-toluenesulfonic acid

→

oil

(3-hydroxyadamantyloxycarbonyl)methyl methacrylate

溶媒

dichloromethane

反応条件

後処理

1. 1
   workup.ADDITIONwas added
2. 2
   温度Then, the mixture was refluxed for 15 hours
3. 3
   その他while removing water
4. 4
   その他After the reaction

実験手順

Hydroxycarbonylmethyl methacrylate (30 g) and dihydroxyadamantane (16.8) were added into dichloromethane (500 ml), and p-toluenesulfonic acid (1 g) was added thereto. Then, the mixture was refluxed for 15 hours while removing water generated. After the reaction, conventional after-treatments were carried out to obtain oil (21.2 g), which was identified to be Monomer A described above.

出典