反応 #3073
ord-dfbffeb92a874b419566deb178159f88
反応条件
詳細条件
See reaction.notes.procedure_details.
後処理
- 1抽出Extraction and chromatography
実験手順
To a Suspension of 1.1 mmol NaH in 5 mL DMF at 0° C. was added a solution of 1.0 mmol tetrazole in 2 mL DMF. After 30 min, trimethylsilylethoxymethylchloride was added and the mixture stirred for 16 h. Extraction and chromatography provided trimethylsilylethoxymethyltetrazole as an oil.