反応 #2931

反応方程式

water

1-(3-Furyl)-1-(4-methyl-5-oxazolyl)ethanol

Trimethylsilylazide

boron trifluoride

→

title compound

1-Azido-1-(3-furyl)-1-(4-methyl-5-oxazolyl)ethane

溶媒

benzene

反応条件

後処理

1. 1
   抽出extracted

実験手順

1-(3-Furyl)-1-(4-methyl-5-oxazolyl)ethanol (1 g) was suspended in benzene (4 ml). Trimethylsilylazide (822 μl) was added followed by boron trifluoride diethyletherate (770 μl). The mixture was stirred overnight at room temperature, then poured into water and extracted to give the title compound.

出典