反応 #2676
ord-3ce42197cace4f5dad3160cf94f08e0c
反応方程式
alcohol
2,3-dichloro-4,5bis-[(2-methoxyethoxy)-methoxy]-styrol
m-chloro perbenzoic acid
→
expected product
収率 99.6%
2,3-dichloro-4,5bis-[(2-methoxyethoxy)-methoxy]-(1,2-epoxy) styrol
収率 99.6%
反応条件
詳細条件
See reaction.notes.procedure_details.
後処理
- 1その他were reacted
実験手順
Using the procedure of Stage D of Example 40, 13.2 g of thee allylic alcohol of Step C and 10.3 g of m-chloro perbenzoic acid were reacted to obtain 13.7 g of the expected product with a Rf=0.25 (AcOEt-cyclohexane 6-4).