反応 #2675

反応方程式

ester

2,3-dichloro-4,5bis-[(2-methoxyethoxy)-methoxy]-styryl carboxylate

diisobutylaluminium hydride

→

expected product

収率 99.6%

2,3-dichloro-4,5bis-[(2-methoxyethoxy)-methoxy]-styrol

収率 99.6%

反応条件

後処理

1. 1
   その他were reacted

実験手順

Using the procedure of Stage C of Example 40, 20 g of ester of Step B and 88 ml of diisobutylaluminium hydride were reacted to obtain 17.9 g of the expected product melting at 60° C.

出典