反応 #2542

ord-b04fe9c2f1da4526a30f3f2067ac49b1

反応方程式

Nc1ccc2c(c1)OCO2
3,4-methylenedioxyaniline
O=C(Cl)c1ccc([N+](=O)[O-])cc1
4-nitrobenzoyl chloride
O=C(Nc1ccc2c(c1)OCO2)c1ccc([N+](=O)[O-])cc1
title compound
収率 87.2%
O=C(Nc1ccc2c(c1)OCO2)c1ccc([N+](=O)[O-])cc1
4-Nitro-N-(3,4-methylenedioxyphenyl)benzamide
収率 87.2%

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

Using 3,4-methylenedioxyaniline (1.44 g, 10.5 mmol) and 4-nitrobenzoyl chloride (1.86 g, 10.0 mmol), the procedure of Reference Example 11 was repeated to obtain 2.49 g (87.2%) of the title compound in the form of yellow crystals.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US05728835uspto-grants-1998_03