反応 #2541

ord-81108896a4f04eedb46c78483e919025

反応方程式

Nc1ccc(Cl)cc1
4-chloroaniline
O=C(O)c1ccc([N+](=O)[O-])cc1
4-nitrobenzoic acid
O=C(Nc1ccc(Cl)cc1)c1ccc([N+](=O)[O-])cc1
title compound
収率 98.7%
O=C(Nc1ccc(Cl)cc1)c1ccc([N+](=O)[O-])cc1
4-Nitro-N-(4-chlorophenyl)benzamide
収率 98.7%

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

Using 4-chloroaniline (1.42 g, 11.0 mmol) and 4-nitrobenzoic acid (1.76 g, 10.4 mmol), the procedure of Reference Example 16 was repeated to obtain 2.84 g (98.5%) of the title compound in the form of yellow crystals.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US05728835uspto-grants-1998_03