反応 #2538
ord-c16cf1c3e2df4892b6f3150e9b21bcaf
反応方程式
3-methylthioaniline
3-nitrobenzoic acid
→
title compound
収率 94.6%
3-Nitro-N-(3-methylthiophenyl)benzamide
収率 94.6%
反応条件
詳細条件
See reaction.notes.procedure_details.
実験手順
Using 3-methylthioaniline (2.1 ml, 16.5 mmol) and 3-nitrobenzoic acid (2.64 g, 15.0 mmol), the procedure of Reference Example 16 was repeated to obtain 4.09 g (94.6%) of the title compound in the form of light yellow needle crystals.