反応 #2522

ord-20a899a14e114ac08ae516cd5bce4b60

反応方程式

Nc1ccccc1
aniline
O=C(O)c1ccc([N+](=O)[O-])cc1
4-nitrobenzoic acid
O=C(Nc1ccccc1)c1ccc([N+](=O)[O-])cc1
title compound
収率 97.5%
O=C(Nc1ccccc1)c1ccc([N+](=O)[O-])cc1
4-Nitro-N-(phenyl)benzamide
収率 97.5%

試薬

なし

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

Using aniline (1.50 ml, 16.5 mmol) and 4-nitrobenzoic acid (1.77 g, 10.5 mmol), the procedure of Reference Example 16 was repeated to obtain 2.48 g (97.5%) of the title compound in the form of colorless powder.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US05728835uspto-grants-1998_03