反応 #2513

ord-a73df83aa26e46b6a84924990ae0f10f

反応方程式

COc1ccccc1N
o-anisidine
O=C(O)c1ccncc1
4-carboxypyridine
COc1ccccc1NC(=O)c1ccncc1
title compound
収率 97.3%
COc1ccccc1NC(=O)c1ccncc1
4-[(2-Methoxyanilino)carbonyl]pyridine
収率 97.3%

試薬

なし

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

Using o-anisidine (2.34 g, 19.0 mmol) and 4-carboxypyridine (2.29 g, 19.0 mmol), the procedure of Reference Example 11 was repeated to obtain 4.22 g (97.2%) of the title compound in the form of colorless powder.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US05728835uspto-grants-1998_03