反応 #2511

ord-e35a3aec1e0643e09ded967995999b79

反応方程式

COc1ccccc1N
o-anisidine
COc1cccc(C(=O)Cl)c1
m-anisoyl chloride
COc1cccc(C(=O)Nc2ccccc2OC)c1
title compound
収率 100.0%
COc1cccc(C(=O)Nc2ccccc2OC)c1
3-Methoxy-N-(2-methoxyphenyl)benzamide
収率 100.0%

試薬

なし

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

Using o-anisidine (1.0 ml, 8.55 mmol) and m-anisoyl chloride (1.2 ml, 8.55 mmol), the procedure of Reference Example 2 was repeated to obtain 2.2 g (100%) of the title compound in the form of brown oil.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US05728835uspto-grants-1998_03