反応 #2507846

ord-98c3198f70774fed8176f88e3b49eb54

反応方程式

O.O.OC[C@H]1O[C@H](O[C@H]2O[C@H](CO)[C@@H](O)[C@H](O)[C@H]2O)[C@H](O)[C@@H](O)[C@@H]1O
trehalose dihydrate
NCC(=O)O
glycine
CC(C[*:1])[*:2]
polypropylene
→
NCC(=O)O.OC[C@H]1O[C@H](O[C@H]2O[C@H](CO)[C@@H](O)[C@H](O)[C@H]2O)[C@H](O)[C@@H](O)[C@@H]1O
Trehalose Glycine

反応物

O.O.OC[C@H]1O[C@H](O[C@H]2O[C@H](CO)[C@@H](O)[C@H](O)[C@H]2O)[C@H](O)[C@@H](O)[C@@H]1O
trehalose dihydrate
NCC(=O)O
glycine
CC(C[*:1])[*:2]
polypropylene

試薬

なし

溶媒

O
water
O
water

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    workup.ADDITIONwas added at room temperature
  2. 2
    その他was obtained
  3. 3
    workup.ADDITIONWithout adding any acid

実験手順

17.84 g of trehalose dihydrate and 4.03 g of glycine were carefully weighed and transferred into a sterile polypropylene bottle, to which 300 ml of purified water was added at room temperature and stirred slowly until a clear solution was obtained. The pH was measured and found to be 5.5. Without adding any acid, the volume was adjusted to 350 ml with purified water. The pH was measured and found to be 5.5.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US07956028B2uspto-grants-2011_06