反応 #2507809

反応方程式

pentacene

maleimide

→

pentacene maleimide

溶媒

dichlorobenzene

反応条件

後処理

1. 1
   温度The mixture is cooled to room temperature
2. 2
   ろ過the precipitate is filtered
3. 3
   洗浄washed with toluene
4. 4
   その他dried
5. 5
   その他Recrystallization from dichlorobenzene

実験手順

A suspension of pentacene (287 mg, 1 mmole) and maleimide (1 mmole) in 4 mL of dichlorobenzene is heated to 160° C. for 4 hours. The mixture is cooled to room temperature and the precipitate is filtered, washed with toluene and dried. Recrystallization from dichlorobenzene affords pure samples of pentacene-maleimide adduct as white needles.

出典