反応 #2506
ord-df69311069264a20a142aa147b4fbb47
反応方程式
o-anisidine
3-nitrobenzenesulfonyl chloride
→
title compound
収率 89.5%
N-(2-Methoxyphenyl)-3-nitrobenzenesulfonamide
収率 89.5%
反応条件
詳細条件
See reaction.notes.procedure_details.
実験手順
Using o-anisidine (1.0 ml, 8.55 mmol) and 3-nitrobenzenesulfonyl chloride (1.95 g, 8.55 mmol), the procedure of Reference Example 2 was repeated to obtain 2.36 g (89.5%) of the title compound in the form of light yellow needle crystals.