反応 #2467947

反応方程式

2-Benzyl-3-(4-phenyl-thiazol-2-ylamino)-propionic ethyl ester

KOH

KHSO4

→

2-Benzyl-3-(4-phenyl-thiazol-2-ylamino)-propionic acid

溶媒

EtOH

water

反応条件

後処理

1. 1
   その他lyophilized before purification

実験手順

To a solution of 2-Benzyl-3-(4-phenyl-thiazol-2-ylamino)-propionic ethyl ester (22r) (0.028 mmol, 10 mg) in EtOH (2 mL) and water (200 μL) is added KOH 1N solution (224 μL, 8 eq.). After 5 hours, the solution is neutralized with KHSO4 1N solution and lyophilized before purification.

出典