反応 #2389089

反応方程式

dodecane thiol

sulfuryl chloride

→

dodecansulfenyl chloride

溶媒

CHCl3

反応条件

後処理

1. 1
   その他Removal of solvent (aspirator)

実験手順

To a solution of dodecane thiol (1.00 mL, 4.17 mmol, Aldrich Chemical Company) in 20 mL CHCl3 was added sulfuryl chloride (0.74 mL, 9.18 mmol, Aldrich Chemical Company), and the resulting mixture was stirred at room temperature for 18 h. Removal of solvent (aspirator), afforded dodecansulfenyl chloride that was determined to be sufficiently pure by 1H NMR.

出典