反応 #2389088

反応方程式

dodecane thiol

chloride

→

dodecansulfenyl chloride

溶媒

CHCl3

反応条件

後処理

1. 1
   その他Removal of solvent (aspirator)

実験手順

To a solution of dodecane thiol (1.00 mL, 4.17 mmol, Aldrich) in 20 mL CHCl3 was added suliryl chloride (0.74 mL, 9.19 mmol, Aldrich), and the regulting mixture was stirred at room temperature for 18 h. Removal of solvent (aspirator), afforded dodecansulfenyl chloride that was determined to be sufficiently pure by 1H NMR.

出典