反応 #2383780

反応方程式

Benzoic acid

2-chloroethyl vinyl ether

sodium hydroxide

triethylamine

→

Benzoyloxyethyl Vinyl Ether

溶媒

toluene

反応条件

実験手順

Benzoic acid (244 g) (2 mol) was dissolved in 3,000 ml of toluene, and thereto were added 320 g of 2-chloroethyl vinyl ether, 88 g of sodium hydroxide, 25 g of tetrabutylammonium bromide, and 100 g of triethylamine. The resulting mixture was stirred with heating at 120° C. for 5 hours.

出典