反応 #2383763

反応方程式

3,4-dimethylpyrazole

formalin

→

solid

収率 95.0%

N-hydroxymethyl-3,4-dimethylpyrazole

収率 95.0%

溶媒

methanol

反応条件

後処理

1. 1
   その他Water and methanol were then evaporated

実験手順

96 g (1.0 mol) of 3,4-dimethylpyrazole in 50 ml of methanol were dissolved in 100 g (1.0 mol) of formalin solution (30%) at room temperature. Water and methanol were then evaporated. The title compound remained as a white solid (yield 95%).

出典