反応 #2358505

反応方程式

DL-valine

N-benzoyl-L-alanine

→

L-valine N-benzoyl-L-alanine

収率 86.4%

溶媒

water

反応条件

後処理

1. 1
   その他to form a clear solution, which
2. 2
   温度was cooled slowly
3. 3
   温度When the solution was cooled to room temperature after 2 hours
4. 4
   その他the precipitated crystals were separated by filtration
5. 5
   洗浄washed with 50 mL of deionized water
6. 6
   その他dried

実験手順

Twenty four grams of DL-valine and 19.3 g of N-benzoyl-L-alanine were suspended in 200 mL of deionized water. The suspension was heated to 95° C. to form a clear solution, which was cooled slowly. When the solution was cooled to room temperature after 2 hours, the precipitated crystals were separated by filtration, washed with 50 mL of deionized water, and dried to obtain 26.8 g of crystalline L-valine N-benzoyl-L-alanine complex (L-valine to N-benzoyl-L-alanine molar ratio of 1:1).

出典