反応 #2355890

反応方程式

di-p-tolylamine

potassium carbonate

dibromobenzo[a]perylene

→

bis(di-p-tolylamino)benzo[a]perylene

溶媒

water

反応条件

後処理

1. 1
   その他This mixture stood still for reaction at 200 degrees centigrade for thirty hours
2. 2
   抽出was extracted by chloroform

実験手順

Then, two equivalents of di-p-tolylamine, potassium carbonate, and copper power were added to the thus obtained dibromobenzo[a]perylene. This mixture stood still for reaction at 200 degrees centigrade for thirty hours. After reactant solution was diluted with water, reactant was extracted by chloroform. Thereafter, the reactant was refined in a conventional manner to thereby obtain bis(di-p-tolylamino)benzo[a]perylene.

出典