反応 #2354235

反応方程式

(4-mercaptophenyl)methanol

5-bromopicolinonitrile

→

title compound

収率 28.4%

5-(4-(hydroxymethyl)phenylthio)picolinonitrile

収率 28.4%

反応条件

実験手順

Using the method of Preparation 155 using (4-mercaptophenyl)methanol (10.0 g, 71.3 mmol) and 5-bromopicolinonitrile (13.0 g, 71.3 mmol) affords the title compound (4.90 g, 28%).): 243 (M+H, 100%).

出典