反応 #2329047

反応方程式

dichlorophthalazine

hydrazine hydrate

→

title compound

(4-Chloro-phthalazin-1-yl)-hydrazine

溶媒

ethanol

反応条件

後処理

1. 1
   ろ過the precipitate is filtered with suction
2. 2
   洗浄rinsed with ethanol

実験手順

10 g commercially available dichlorophthalazine are added portionwise at 90° C. to a solution of 50 ml ethanol and 20 ml hydrazine hydrate. After 10 min the reaction mixture is cooled to ambient temperature, the precipitate is filtered with suction and rinsed with ethanol to yield 8.4 g of the title compound.

出典