反応 #2329041

反応方程式

4-dodecyloxybenzyl chloride

thionyl chloride

4-tetradecyloxybenzyl alcohol

→

4-Tetradecyloxybenzyl Chloride

溶媒

CH2Cl2

反応条件

後処理

1. 1
   その他This one was synthesized

実験手順

This one was synthesized following the same general procedure as that for the preparation of 4-dodecyloxybenzyl chloride; thionyl chloride (7.45 g, 63.1 mmol), 4-tetradecyloxybenzyl alcohol (18.4 g, 57.4 mmol), CH2Cl2 (150 mL). 16.28 g (84%) white solid which decomposes upon melting.

出典