反応 #2329040
ord-a033880df3c848cfbf8807a3cf38d580
反応方程式
4-dodecyloxybenzyl chloride
thionyl chloride
4-decyloxybenzyl alcohol
→
4-Decyloxybenzyl Chloride
溶媒
反応条件
詳細条件
See reaction.notes.procedure_details.
後処理
- 1その他Was synthesized
実験手順
Was synthesized following the same general procedure as that for the preparation of 4-dodecyloxybenzyl chloride; thionyl chloride (5.00 g, 42.4 mmol), 4-decyloxybenzyl alcohol (10.2 g, 38.6 mmol), CH2Cl2 (100 mL). 9.87 g (90%) white solid which decomposes upon melting.