反応 #2329038

ord-2efc181edf924ec9a8b065fcbc3c2897

反応方程式

CCOc1ccc(CCl)cc1
4-ethoxybenzyl chloride
O=S(Cl)Cl
thionyl chloride
CCCCCCCCOc1ccc(CO)cc1
4-octyloxybenzyl alcohol
CCCCCCCCOc1ccc(CCl)cc1
4-Octyloxybenzyl Chloride

溶媒

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他This compound was synthesized

実験手順

This compound was synthesized following the same general procedure as that for the preparation of 4-ethoxybenzyl chloride; thionyl chloride (6.36 g, 53.4 mmol), 4-octyloxybenzyl alcohol (12.4 g, 52.5 mmol), CH2Cl2 (150 mL).

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US07671033B2uspto-grants-2010_03