反応 #2329032

反応方程式

N-ethoxycarbonyl phthalimide

H2O

→

2-(2-Phthalimidoethylamino)ethanol

反応条件

後処理

1. 1
   洗浄the solid product washed with methanol (40 ml)
2. 2
   その他The remaining white solid (Compound 14) was collected
3. 3
   その他dried

実験手順

10.4 g (0.1 mol) of N,N-(2-hydroxyethyl),ethyl amine and 22 g (0.1 mol) of N-ethoxycarbonyl phthalimide were dissolved in 50 ml of H2O and stirred for 2 hours. The reaction mixture was lyophilized and the solid product washed with methanol (40 ml). The remaining white solid (Compound 14) was collected and dried.

出典