反応 #2328999

反応方程式

tert-butyl [5-(6-methoxy-1,3-benzoxazol-2-yl)pyridin-2-yl]carbamate

5-(6-methoxy-1,3-benzoxazol-2-yl)pyrimidin-2-amine

→

title intermediate

tert-Butyl [5-(6-methoxy-1,3-benzoxazol-2-yl)pyrimidin-2-yl]carbamate

反応条件

後処理

1. 1
   その他to give 115 mg

実験手順

The title intermediate was synthesized from 5-(6-methoxy-1,3-benzoxazol-2-yl)pyrimidin-2-amine according to the procedure described for tert-butyl [5-(6-methoxy-1,3-benzoxazol-2-yl)pyridin-2-yl]carbamate to give 115 mg. 1H NMR 400 MHz, Chloroform-d) δ ppm 9.33 (s, 2H) 8.17 (s, 1H) 7.65 (d, 1H) 7.14 (d, 1H) 7.00 (dd, 1 H) 3.90 (s, 3H) 1.60 (s, 9H). MS m/z 343 (M+H).

出典