反応 #2328992

反応方程式

2-[6-(dimethylamino)pyridin-3-yl]-1,3-benzoxazol-5-ol

5-(6-Methoxy-1,3-benzoxazol-2-yl)-N,N-dimethylpyrimidin-2-amine

→

title compound

2-[2-(Dimethylamino)pyrimidin-5-yl]-1,3-benzoxazol-6-ol

反応条件

後処理

1. 1
   その他to give 30.3 mg

実験手順

The title compound was synthesized from 5-(6-Methoxy-1,3-benzoxazol-2-yl)-N,N-dimethylpyrimidin-2-amine according to the general procedure as described for 2-[6-(dimethylamino)pyridin-3-yl]-1,3-benzoxazol-5-ol to give 30.3 mg: 1H NMR δ ppm 9.85 (br. s, 1H) 8.97 (s, 2H) 7.51 (d, 1H) 7.05 (d, 1H) 6.82 (dd, 1H) 3.22 (s, 6 H); MS m/z 257 (M+H).

出典