反応 #2320091

ord-d66416cdec7742b6ade4073c600df31f

反応方程式

Fc1ccc(N2CCNCC2)cc1C(F)(F)F
1-(4-fluoro-3-trifluoromethyl-phenyl)-piperazine
CCCBr
1-bromopropane
CCCN1CCN(c2ccc(F)c(C(F)(F)F)c2)CC1
1-(4-Fluoro-3-trifluoromethyl-phenyl)-4-propyl-piperazine

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他the title compound was recovered by the procedure

実験手順

Beginning with 1-(4-fluoro-3-trifluoromethyl-phenyl)-piperazine and 1-bromopropane, the title compound was recovered by the procedure described in Example 2. m.p. 238° C. (HCl); MS m/z (rel. intensity, 70 eV) 290 (M+, 17), 261 (70), 190 (34), 70 (bp), 56 (44).

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: USRE041315E1uspto-grants-2010_05